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Information card for entry 4108852
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Coordinates | 4108852.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | meso-1,1,4,4-Tetrakis[bis(trimethylsilyl)methyl]- 3,4-dicyano-1,4-diisopropyltetrasilane |
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Formula | C36 H92 N2 Si12 |
Calculated formula | C36 H92 N2 Si12 |
SMILES | C[Si](C([Si](C([Si](C)(C)C)[Si](C)(C)C)([Si@H](C#N)[Si@H](C#N)[Si](C([Si](C)(C)C)[Si](C)(C)C)(C([Si](C)(C)C)[Si](C)(C)C)C(C)C)C(C)C)[Si](C)(C)C)(C)C |
Title of publication | Reactivity of the Disilyne RSi\τbSiR (R = SiiPr[CH(SiMe3)2]2) toward Silylcyanide: Two Pathways To Form the Bis-Adduct [RSiSiR(CNSiMe3)2] with Some Silaketenimine Character and a 1,4-Diaza-2,3-disilabenzene Analogue |
Authors of publication | Katsuhiko Takeuchi; Masaaki Ichinohe; Akira Sekiguchi |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 16848 - 16849 |
a | 9.627 ± 0.0005 Å |
b | 10.958 ± 0.0003 Å |
c | 14.608 ± 0.0008 Å |
α | 105.456 ± 0.003° |
β | 95.914 ± 0.003° |
γ | 110.091 ± 0.003° |
Cell volume | 1362.31 ± 0.12 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0492 |
Residual factor for significantly intense reflections | 0.0432 |
Weighted residual factors for significantly intense reflections | 0.1183 |
Weighted residual factors for all reflections included in the refinement | 0.123 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4108852.html
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