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Information card for entry 4108964
Preview
Coordinates | 4108964.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H43 Fe O P Si |
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Calculated formula | C25 H43 Fe O P Si |
SMILES | [Fe]12345([P]([Si]1(C)C)(C1CCCCC1)C1CCCCC1)(C#[O])[c]1([c]2([c]3([c]4([c]51C)C)C)C)C |
Title of publication | Recombination of an Fe-Si-P Linkage to an Fe-P-Si Linkage through an Isolable Intermediate Phosphasilaferracyclopropane |
Authors of publication | Masaaki Okazaki; Takahiko Yoshitomi; Junpei Naito; Akira Sato; Takashi Komuro; Hiromi Tobita |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 17674 - 17675 |
a | 14.7697 ± 0.0004 Å |
b | 15.3225 ± 0.0005 Å |
c | 11.5537 ± 0.0004 Å |
α | 90° |
β | 98.5242 ± 0.0007° |
γ | 90° |
Cell volume | 2585.82 ± 0.14 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0392 |
Residual factor for significantly intense reflections | 0.0321 |
Weighted residual factors for significantly intense reflections | 0.0852 |
Weighted residual factors for all reflections included in the refinement | 0.0932 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.244 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4108964.html
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Users of the data should acknowledge the original authors of the
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