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Information card for entry 4112093
Preview
Coordinates | 4112093.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Dipp*Ge(PhCNNCPh)GeDipp*.0.65PhCN.0.35MeCyclopentane.0.5Et2O |
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Formula | C83.65 H98.45 Ge2 N2.65 |
Calculated formula | C83.65 H98.45 Ge2 N2.65 |
Title of publication | Reactions of the Heavier Group 14 Element Alkyne Analogues Ar'EEAr' (Ar' = C6H3-2,6(C6H3-2,6-Pri2)2; E = Ge, Sn) with Unsaturated Molecules: Probing the Character of the EE Multiple Bonds |
Authors of publication | Chunming Cui; Marilyn M. Olmstead; James C. Fettinger; Geoffrey H. Spikes; Philip P. Power |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2005 |
Journal volume | 127 |
Pages of publication | 17530 - 17541 |
a | 13.089 ± 0.0017 Å |
b | 14.2078 ± 0.0017 Å |
c | 21.234 ± 0.003 Å |
α | 93.795 ± 0.003° |
β | 91.656 ± 0.003° |
γ | 115.63 ± 0.003° |
Cell volume | 3545.2 ± 0.8 Å3 |
Cell temperature | 93 ± 2 K |
Ambient diffraction temperature | 93 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0753 |
Residual factor for significantly intense reflections | 0.0468 |
Weighted residual factors for significantly intense reflections | 0.1155 |
Weighted residual factors for all reflections included in the refinement | 0.1317 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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