Crystallography Open Database

Information card for entry 4112382

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Coordinates	4112382.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H39 Cl P2 Si W
Calculated formula	C23 H39 Cl P2 Si W
Title of publication	Synthons for Coordinatively Unsaturated Complexes of Tungsten, and Their Use for the Synthesis of High Oxidation-State Silylene Complexes
Authors of publication	Benjamin V. Mork; T. Don Tilley
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	4375 - 4385
a	17.2867 ± 0.0002 Å
b	9.2357 ± 0.0002 Å
c	17.8766 ± 0.0004 Å
α	90°
β	115.65 ± 0.001°
γ	90°
Cell volume	2572.83 ± 0.09 Å³
Cell temperature	273.2 K
Ambient diffraction temperature	142 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/a 1
Hall space group symbol	-P 2yab
Residual factor for all reflections	0.0847
Residual factor for significantly intense reflections	0.0517
Weighted residual factors for all reflections	0.0664
Weighted residual factors for significantly intense reflections	0.0599
Weighted residual factors for all reflections included in the refinement	0.0599
Goodness-of-fit parameter for all reflections included in the refinement	1.626
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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