Crystallography Open Database

Information card for entry 4112383

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Coordinates	4112383.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H50 P2 Si W
Calculated formula	C35 H50 P2 Si W
Title of publication	Synthons for Coordinatively Unsaturated Complexes of Tungsten, and Their Use for the Synthesis of High Oxidation-State Silylene Complexes
Authors of publication	Benjamin V. Mork; T. Don Tilley
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	4375 - 4385
a	18.3293 ± 0.0001 Å
b	17.9586 ± 0.0004 Å
c	20.499 ± 0.0001 Å
α	90°
β	90°
γ	90°
Cell volume	6747.63 ± 0.16 Å³
Cell temperature	168 K
Ambient diffraction temperature	168 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0868
Residual factor for significantly intense reflections	0.0234
Weighted residual factors for all reflections	0.0366
Weighted residual factors for significantly intense reflections	0.0222
Weighted residual factors for all reflections included in the refinement	0.0222
Goodness-of-fit parameter for all reflections included in the refinement	0.646
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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