Information card for entry 4113168

Structure parameters

• Formula: C18 H39 P2 Re
• Calculated formula: C18 H39 P2 Re
• Title of publication: Synthesis and Reactivity of the Hydrido- and Alkylrhenium Methylidene Complexes Cp*(PMe3)2(R)ReCH2 (R = H, CH3)
• Authors of publication: Jennifer R. Krumper; Richard L. Martin; P. Jeffrey Hay; Cathleen M. Yung; John Veltheer; Robert G. Bergman
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 14804 - 14815
• a: 17.4197 ± 0.0004 Å
• b: 14.6308 ± 0.0003 Å
• c: 32.8142 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8363.2 ± 0.3 ų
• Cell temperature: 163.2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for all reflections included in the refinement: 0.0394
• Goodness-of-fit parameter for all reflections included in the refinement: 1.559
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No