Crystallography Open Database

Information card for entry 4113169

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Coordinates	4113169.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H50 B F24 P2 Re
Calculated formula	C50 H50 B F24 P2 Re
Title of publication	Synthesis and Reactivity of the Hydrido- and Alkylrhenium Methylidene Complexes Cp*(PMe3)2(R)ReCH2 (R = H, CH3)
Authors of publication	Jennifer R. Krumper; Richard L. Martin; P. Jeffrey Hay; Cathleen M. Yung; John Veltheer; Robert G. Bergman
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	14804 - 14815
a	12.2338 ± 0.0003 Å
b	12.9077 ± 0.0003 Å
c	18.1496 ± 0.0004 Å
α	102.179 ± 0.001°
β	93.149 ± 0.001°
γ	96.009 ± 0.001°
Cell volume	2777.35 ± 0.11 Å³
Cell temperature	170.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0
Weighted residual factors for all reflections included in the refinement	0.047
Goodness-of-fit parameter for all reflections included in the refinement	1.929
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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