Information card for entry 4114482

Structure parameters

• Formula: C78 H60 N6 Os P3 Re5 Se8
• Calculated formula: C78 H57 N6 Os1.02 P3 Re4.98 Se8
• Title of publication: Cluster-to-Metal Magnetic Coupling: Synthesis and Characterization of 25-Electron [Re6-nOsnSe8(CN)6](5-n)- (n = 1, 2) Clusters and {Re6-nOsnSe8[CNCu(Me6tren)]6}9+ (n = 0, 1, 2) Assemblies
• Authors of publication: Eric G. Tulsky; Nathan R. M. Crawford; Stéphane A. Baudron; Patrick Batail; Jeffrey R. Long
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 15543 - 15553
• a: 13.176 ± 0.0003 Å
• b: 13.4661 ± 0.0003 Å
• c: 23.1766 ± 0.0005 Å
• α: 91.591 ± 0.001°
• β: 91.104 ± 0.001°
• γ: 104.474 ± 0.001°
• Cell volume: 3978.7 ± 0.15 ų
• Cell temperature: 159 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0732
• Residual factor for significantly intense reflections: 0.0408
• Weighted residual factors for all reflections: 0.0946
• Weighted residual factors for significantly intense reflections: 0.0878
• Goodness-of-fit parameter for all reflections: 0.903
• Goodness-of-fit parameter for significantly intense reflections: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No