Information card for entry 4114483

Structure parameters

• Formula: C57 H46 N7 O Os2 P2 Re4 Se8
• Calculated formula: C59 H20 N7 O Os1.98 P2 Re4.02 Se8
• Title of publication: Cluster-to-Metal Magnetic Coupling: Synthesis and Characterization of 25-Electron [Re6-nOsnSe8(CN)6](5-n)- (n = 1, 2) Clusters and {Re6-nOsnSe8[CNCu(Me6tren)]6}9+ (n = 0, 1, 2) Assemblies
• Authors of publication: Eric G. Tulsky; Nathan R. M. Crawford; Stéphane A. Baudron; Patrick Batail; Jeffrey R. Long
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 15543 - 15553
• a: 12.1936 ± 0.0004 Å
• b: 19.5516 ± 0.0005 Å
• c: 27.723 ± 0.0003 Å
• α: 90°
• β: 102.688 ± 0.001°
• γ: 90°
• Cell volume: 6447.9 ± 0.3 ų
• Cell temperature: 131 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0954
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for all reflections: 0.1124
• Weighted residual factors for significantly intense reflections: 0.0997
• Goodness-of-fit parameter for all reflections: 0.916
• Goodness-of-fit parameter for significantly intense reflections: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No