Information card for entry 4114733

Structure parameters

• Formula: C38 H55 Cl2 Hf Sn
• Calculated formula: C40 H55 Cl Hf Sn
• Title of publication: A New Mechanism for Metal-Catalyzed Stannane Dehydrocoupling Based on α-H-Elimination in a Hafnium Hydrostannyl Complex
• Authors of publication: Nathan R. Neale; T. Don Tilley
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 3802 - 3803
• a: 11.05 ± 0.0003 Å
• b: 13.1794 ± 0.0003 Å
• c: 14.4436 ± 0.0003 Å
• α: 105.362 ± 0.001°
• β: 92.979 ± 0.001°
• γ: 114.077 ± 0.001°
• Cell volume: 1820.98 ± 0.08 ų
• Cell temperature: 273.2 K
• Ambient diffraction temperature: 273.2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for all reflections: 0
• Weighted residual factors for significantly intense reflections: 0.0398
• Goodness-of-fit parameter for all reflections included in the refinement: 1.296
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No