Crystallography Open Database

Information card for entry 4114734

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Coordinates	4114734.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Gd4 H24 Mo12 O60
Calculated formula	Gd4 Mo12 O54
Title of publication	Hydrothermal Assembly of a Novel Three-Dimensional Framework Formed by [GdMo12O42]9- Anions and Nine Coordinated GdIII Cations
Authors of publication	Chuan-De Wu; Can-Zhong Lu; Hong-Hui Zhuang; Jin-Shun Huang
Journal of publication	Journal of the American Chemical Society
Year of publication	2002
Journal volume	124
Pages of publication	3836 - 3837
a	17.2627 ± 0.0005 Å
b	17.2627 ± 0.0005 Å
c	25.6138 ± 0.0008 Å
α	90°
β	90°
γ	120°
Cell volume	6610.3 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	167
Hermann-Mauguin space group symbol	R -3 c :H
Hall space group symbol	-R 3 2"c
Residual factor for significantly intense reflections	0.0467
Weighted residual factors for significantly intense reflections	0.1124
Weighted residual factors for all reflections included in the refinement	0.1209
Goodness-of-fit parameter for all reflections included in the refinement	1.105
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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