Information card for entry 4114912

Structure parameters

• Formula: Cs2 H5.4 O13.7 Si4 V
• Calculated formula: Cs1.996 O13.7013 Si4 V
• Title of publication: Open-Framework and Microporous Vanadium Silicates
• Authors of publication: Xiqu Wang; Lumei Liu; Allan J. Jacobson
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 7812 - 7820
• a: 13.392 ± 0.0018 Å
• b: 13.392 ± 0.0018 Å
• c: 21.568 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3349.9 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.1448
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.0687
• Weighted residual factors for all reflections included in the refinement: 0.0847
• Goodness-of-fit parameter for all reflections included in the refinement: 0.879
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No