Information card for entry 4114913

Structure parameters

• Formula: H6 O14 Rb2 Si4 V
• Calculated formula: O13.8833 Rb1.996 Si4.004 V
• Title of publication: Open-Framework and Microporous Vanadium Silicates
• Authors of publication: Xiqu Wang; Lumei Liu; Allan J. Jacobson
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 7812 - 7820
• a: 13.2878 ± 0.0008 Å
• b: 13.2878 ± 0.0008 Å
• c: 21.256 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3250.3 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.1475
• Residual factor for significantly intense reflections: 0.1109
• Weighted residual factors for significantly intense reflections: 0.3551
• Weighted residual factors for all reflections included in the refinement: 0.3725
• Goodness-of-fit parameter for all reflections included in the refinement: 1.113
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No