Information card for entry 4115032

Structure parameters

• Formula: C24 H38 Br P Pd
• Calculated formula: C24 H2 Br P Pd
• Title of publication: Synthesis, Characterization, and Reactivity of Monomeric, Arylpalladium Halide Complexes with a Hindered Phosphine as the Only Dative Ligand
• Authors of publication: James P. Stambuli; Michael Bühl; John F. Hartwig
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 9346 - 9347
• a: 11.2935 ± 0.0005 Å
• b: 18.229 ± 0.001 Å
• c: 12.044 ± 0.0005 Å
• α: 90°
• β: 112.187 ± 0.003°
• γ: 90°
• Cell volume: 2295.9 ± 0.19 ų
• Cell temperature: 183.2 K
• Ambient diffraction temperature: 183.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0679
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for all reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0325
• Goodness-of-fit parameter for all reflections: 1.36
• Goodness-of-fit parameter for significantly intense reflections: 1.434
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No