Information card for entry 4115033

Structure parameters

• Formula: C20 H36 I P Pd
• Calculated formula: C20 I P Pd
• Title of publication: Synthesis, Characterization, and Reactivity of Monomeric, Arylpalladium Halide Complexes with a Hindered Phosphine as the Only Dative Ligand
• Authors of publication: James P. Stambuli; Michael Bühl; John F. Hartwig
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 9346 - 9347
• a: 15.2945 ± 0.0004 Å
• b: 14.244 ± 0.0004 Å
• c: 20.5478 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4476.4 ± 0.2 ų
• Cell temperature: 183.2 K
• Ambient diffraction temperature: 183.2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for all reflections included in the refinement: 0.0273
• Goodness-of-fit parameter for all reflections included in the refinement: 1.264
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No