Information card for entry 4115707

Structure parameters

• Formula: C16 H31 Cl P2 W
• Calculated formula: C16 H30 Cl P2 W
• Title of publication: High Oxidation-State (Formally d0) Tungsten Silylene Complexes via Double Si-H Bond Activation
• Authors of publication: Benjamin V. Mork; T. Don Tilley
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 9702 - 9703
• a: 8.72 ± 0.0002 Å
• b: 16.612 ± 0.0003 Å
• c: 13.944 ± 0.0001 Å
• α: 90°
• β: 102.536 ± 0.001°
• γ: 90°
• Cell volume: 1971.73 ± 0.06 ų
• Cell temperature: 169.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for all reflections included in the refinement: 0.0371
• Goodness-of-fit parameter for all reflections included in the refinement: 1.411
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No