Information card for entry 4115725

Structure parameters

• Formula: C26 H36 P Y
• Calculated formula: C23 H2.5 P0.5 Y0.5
• Title of publication: Intramolecular Hydrophosphination/Cyclization of Phosphinoalkenes and Phosphinoalkynes Catalyzed by Organolanthanides: Scope, Selectivity, and Mechanism
• Authors of publication: Michael R. Douglass; Charlotte L. Stern; Tobin J. Marks
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 10221 - 10238
• a: 11.1734 ± 0.0012 Å
• b: 11.1734 ± 0.0012 Å
• c: 19.129 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2388.2 ± 0.5 ų
• Cell temperature: 153.2 K
• Ambient diffraction temperature: 153.2 K
• Number of distinct elements: 4
• Space group number: 84
• Hermann-Mauguin space group symbol: P 42/m
• Hall space group symbol: -P 4c
• Residual factor for all reflections: 0.204
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for all reflections: 0.165
• Weighted residual factors for all reflections included in the refinement: 0.138
• Goodness-of-fit parameter for all reflections included in the refinement: 3.2
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No