Information card for entry 4116233

Structure parameters

• Formula: C32 H72 Li4 O8 Rb4
• Calculated formula: C32 H72 Li4 O8 Rb4
• Title of publication: A Remarkable Isostructural Homologous Series of Mixed Lithium-Heavier Alkali Metaltert-Butoxides [(t-BuO)8Li4M4] (M = Na, K, Rb or Cs)
• Authors of publication: David R. Armstrong; William Clegg; Allison M. Drummond; Stephen T. Liddle; Robert E. Mulvey
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2000
• Journal volume: 122
• Pages of publication: 11117 - 11124
• a: 11.705 ± 0.003 Å
• b: 17.07 ± 0.005 Å
• c: 12.957 ± 0.005 Å
• α: 90 ± 0.002°
• β: 110.347 ± 0.019°
• γ: 90 ± 0.002°
• Cell volume: 2427.3 ± 1.4 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 5
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.0976
• Weighted residual factors for all reflections included in the refinement: 0.1088
• Goodness-of-fit parameter for all reflections included in the refinement: 0.904
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No