Crystallography Open Database

Information card for entry 4116234

Preview

Coordinates	4116234.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H72 Cs4 Li4 O8
Calculated formula	C32 H72 Cs4 Li4 O8
Title of publication	A Remarkable Isostructural Homologous Series of Mixed Lithium-Heavier Alkali Metaltert-Butoxides [(t-BuO)8Li4M4] (M = Na, K, Rb or Cs)
Authors of publication	David R. Armstrong; William Clegg; Allison M. Drummond; Stephen T. Liddle; Robert E. Mulvey
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	11117 - 11124
a	12.106 ± 0.003 Å
b	17.08 ± 0.004 Å
c	12.913 ± 0.0017 Å
α	90°
β	109.541 ± 0.013°
γ	90°
Cell volume	2516.2 ± 0.9 Å³
Cell temperature	160 ± 2 K
Ambient diffraction temperature	160 ± 2 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0323
Residual factor for significantly intense reflections	0.023
Weighted residual factors for significantly intense reflections	0.0595
Weighted residual factors for all reflections included in the refinement	0.0625
Goodness-of-fit parameter for all reflections included in the refinement	1.072
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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