Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4116380
Preview
Coordinates | 4116380.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | [tetrakis[u3-(bis(diphenylmethylphposphine)palladium)] tetraantimony] bis[diphenyldidichloroantimony] |
---|---|
Formula | C130 H128 Cl4 O0.5 P8 Pd4 Sb6 |
Calculated formula | C130 H128 Cl4 O0.5 P8 Pd4 Sb6 |
Title of publication | Different Ways To Distort a Tetracapped Tetrahedron on Route to Forming an E4M4 Cubane: The Case of [E4(Pd(PPh2Me)2)4][Ph2EX2]2 (E = Sb, X = Cl; E = Bi, X = Br) |
Authors of publication | Joseph L. Stark; Brian Harms; Ilse Guzman-Jimenez; Kenton H. Whitmire; Régis Gautier; Jean-François Halet; Jean-Yves Saillard |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 1999 |
Journal volume | 121 |
Pages of publication | 4409 - 4418 |
a | 14.176 ± 0.003 Å |
b | 14.77 ± 0.003 Å |
c | 32.465 ± 0.007 Å |
α | 85.08 ± 0.03° |
β | 77.96 ± 0.03° |
γ | 85.23 ± 0.03° |
Cell volume | 6609 ± 3 Å3 |
Cell temperature | 223 ± 2 K |
Ambient diffraction temperature | 223 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0502 |
Residual factor for significantly intense reflections | 0.0386 |
Weighted residual factors for all reflections | 0.1334 |
Weighted residual factors for significantly intense reflections | 0.1206 |
Goodness-of-fit parameter for all reflections | 1.108 |
Goodness-of-fit parameter for significantly intense reflections | 1.133 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4116380.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.