Information card for entry 4116379

Structure parameters

• Chemical name: [( 3-(Bis(diphenylmethylphosphine)palldium)-tetrabismuth][Dibromo- diphenyl bismuth]
• Formula: C128 H124 Bi6 Br4 P8 Pd4
• Calculated formula: C128 H124 Bi6 Br4 P8 Pd4
• Title of publication: Different Ways To Distort a Tetracapped Tetrahedron on Route to Forming an E4M4 Cubane: The Case of [E4(Pd(PPh2Me)2)4][Ph2EX2]2 (E = Sb, X = Cl; E = Bi, X = Br)
• Authors of publication: Joseph L. Stark; Brian Harms; Ilse Guzman-Jimenez; Kenton H. Whitmire; Régis Gautier; Jean-François Halet; Jean-Yves Saillard
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1999
• Journal volume: 121
• Pages of publication: 4409 - 4418
• a: 14.395 ± 0.003 Å
• b: 14.974 ± 0.003 Å
• c: 32.363 ± 0.007 Å
• α: 84.75 ± 0.03°
• β: 77.78 ± 0.03°
• γ: 85.59 ± 0.03°
• Cell volume: 6777 ± 3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1249
• Residual factor for significantly intense reflections: 0.055
• Weighted residual factors for all reflections: 0.1658
• Weighted residual factors for significantly intense reflections: 0.1358
• Goodness-of-fit parameter for all reflections: 1.039
• Goodness-of-fit parameter for significantly intense reflections: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No