Crystallography Open Database

Information card for entry 4117168

Preview

Coordinates	4117168.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H60 Br2 Cl8 Mo2 N4 O4 P4 Pd2
Calculated formula	C288 H240 Br8 Cl32 Mo8 N16 O16 P16 Pd8
Title of publication	Reductive Formation of Straight Linear Metal-Metal Bonded Tetranuclear Complexes X-M-Mo-Mo-M-X from X2M...Mo-Mo...MX2 Supported by Four Tridentate 6-Diphenylphosphino-2-pyridonate Ligands (M = Pd, Pt; X = Cl, Br, I)
Authors of publication	Kazushi Mashima; Hiroshi Nakano; Akira Nakamura
Journal of publication	Journal of the American Chemical Society
Year of publication	1996
Journal volume	118
Pages of publication	9083 - 9095
a	17.455 ± 0.003 Å
b	17.4548 Å
c	25.971 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	7913 ± 2 Å³
Cell temperature	23 K
Ambient diffraction temperature	23 K
Number of distinct elements	9
Space group number	80
Hermann-Mauguin space group symbol	I 41
Hall space group symbol	I 4bw
Residual factor for significantly intense reflections	0.029
Weighted residual factors for significantly intense reflections	0.027
Goodness-of-fit parameter for significantly intense reflections	2.09
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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