Information card for entry 4117169

Structure parameters

• Formula: C69 H54 Cl2 I2 Mo2 N4 O4 P4 Pd2
• Calculated formula: C276 H216 Cl8 I8 Mo8 N16 O16 P16 Pd8
• Title of publication: Reductive Formation of Straight Linear Metal-Metal Bonded Tetranuclear Complexes X-M-Mo-Mo-M-X from X2M...Mo-Mo...MX2 Supported by Four Tridentate 6-Diphenylphosphino-2-pyridonate Ligands (M = Pd, Pt; X = Cl, Br, I)
• Authors of publication: Kazushi Mashima; Hiroshi Nakano; Akira Nakamura
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1996
• Journal volume: 118
• Pages of publication: 9083 - 9095
• a: 16.074 ± 0.007 Å
• b: 16.807 ± 0.007 Å
• c: 28.194 ± 0.004 Å
• α: 90°
• β: 94.97 ± 0.02°
• γ: 90°
• Cell volume: 7588 ± 5 ų
• Cell temperature: 23 K
• Ambient diffraction temperature: 23 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.068
• Weighted residual factors for significantly intense reflections: 0.084
• Goodness-of-fit parameter for significantly intense reflections: 5.3
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No