Information card for entry 4119803

Structure parameters

• Formula: C42 H72 P2 Pd Si8 Sn
• Calculated formula: C42 H72 P2 Pd Si8 Sn
• SMILES: [Pd]12([Sn]3([Si]([Si]([Si]([Si]23[Si](C)(C)C)(C)C)(C)C)([Si](C)(C)C)[Si](C)(C)C)[Si](C)(C)C)[P](CC[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Coordination Chemistry of Disilylated Stannylenes with Group 10 d10 Transition Metals: Silastannene vs Stannylene Complexation
• Authors of publication: Henning Arp; Christoph Marschner; Judith Baumgartner; Patrick Zark; Thomas Müller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 7949 - 7959
• a: 12.226 ± 0.002 Å
• b: 13.613 ± 0.003 Å
• c: 20.105 ± 0.004 Å
• α: 71.61 ± 0.03°
• β: 74.94 ± 0.03°
• γ: 87.72 ± 0.03°
• Cell volume: 3062.9 ± 1.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1293
• Residual factor for significantly intense reflections: 0.0977
• Weighted residual factors for significantly intense reflections: 0.2212
• Weighted residual factors for all reflections included in the refinement: 0.2371
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No