Information card for entry 4119804

Structure parameters

• Formula: C32 H88 K N O2 Si10 Sn
• Calculated formula: C32 H88 K N O2 Si10 Sn
• SMILES: [Sn](N([Si](C)(C)C)[Si](C)(C)C)([Si]([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)[Si]([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C.[K]([O]1CCCC1)[O]1CCCC1
• Title of publication: Coordination Chemistry of Disilylated Stannylenes with Group 10 d10 Transition Metals: Silastannene vs Stannylene Complexation
• Authors of publication: Henning Arp; Christoph Marschner; Judith Baumgartner; Patrick Zark; Thomas Müller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 7949 - 7959
• a: 12.108 ± 0.002 Å
• b: 21.981 ± 0.004 Å
• c: 20.554 ± 0.004 Å
• α: 90°
• β: 98.9 ± 0.03°
• γ: 90°
• Cell volume: 5404.5 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1139
• Residual factor for significantly intense reflections: 0.0994
• Weighted residual factors for significantly intense reflections: 0.1711
• Weighted residual factors for all reflections included in the refinement: 0.1765
• Goodness-of-fit parameter for all reflections included in the refinement: 1.38
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No