Information card for entry 4120283

Structure parameters

• Formula: C77 H157 K N O22 Si5 U
• Calculated formula: C77 H157 K N O22 Si5 U
• Title of publication: Tuning Uranium-Nitrogen Multiple Bond Formation with Ancillary Siloxide Ligands
• Authors of publication: Clément Camp; Jacques Pécaut; Marinella Mazzanti
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 12101 - 12111
• a: 14.047 ± 0.0008 Å
• b: 14.047 ± 0.0008 Å
• c: 43.104 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 7365.7 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 145
• Hermann-Mauguin space group symbol: P 32
• Hall space group symbol: P 32
• Residual factor for all reflections: 0.0989
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for significantly intense reflections: 0.1083
• Weighted residual factors for all reflections included in the refinement: 0.1232
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No