Crystallography Open Database

Information card for entry 4120284

4120283 << 4120284 >> 4120285

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Coordinates	4120284.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H139 K N4 O18 Si5 U
Calculated formula	C68 H139 K N4 O18 Si5 U
Title of publication	Tuning Uranium-Nitrogen Multiple Bond Formation with Ancillary Siloxide Ligands
Authors of publication	Clément Camp; Jacques Pécaut; Marinella Mazzanti
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	12101 - 12111
a	13.7947 ± 0.0003 Å
b	26.1912 ± 0.0007 Å
c	25.0278 ± 0.0005 Å
α	90°
β	93.479 ± 0.002°
γ	90°
Cell volume	9025.9 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0765
Residual factor for significantly intense reflections	0.0449
Weighted residual factors for significantly intense reflections	0.0941
Weighted residual factors for all reflections included in the refinement	0.1074
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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