Information card for entry 4120285

Structure parameters

• Formula: C67 H140 K N3 O22 Si4 U
• Calculated formula: C67 H140 K N3 O22 Si4 U
• Title of publication: Tuning Uranium-Nitrogen Multiple Bond Formation with Ancillary Siloxide Ligands
• Authors of publication: Clément Camp; Jacques Pécaut; Marinella Mazzanti
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 12101 - 12111
• a: 14.0305 ± 0.0005 Å
• b: 24.7215 ± 0.0007 Å
• c: 26.3108 ± 0.0009 Å
• α: 90°
• β: 98.009 ± 0.003°
• γ: 90°
• Cell volume: 9037 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.075
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.12
• Weighted residual factors for all reflections included in the refinement: 0.1287
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No