Information card for entry 4120740

Structure parameters

• Formula: C26 H59 N3 O Si6 U
• Calculated formula: C26 H59 N3 O Si6 U
• Title of publication: Stable Uranium(VI) Methyl and Acetylide Complexes and the Elucidation of an Inverse Trans Influence Ligand Series
• Authors of publication: Andrew J. Lewis; Patrick J. Carroll; Eric J. Schelter
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 13185 - 13192
• a: 12.3823 ± 0.0008 Å
• b: 12.1284 ± 0.0007 Å
• c: 13.0025 ± 0.0008 Å
• α: 90°
• β: 92.667 ± 0.003°
• γ: 90°
• Cell volume: 1950.6 ± 0.2 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.035
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0973
• Weighted residual factors for all reflections included in the refinement: 0.0973
• Goodness-of-fit parameter for all reflections included in the refinement: 1.577
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No