Information card for entry 4120741

Structure parameters

• Formula: C19 H57 N3 Si6 U
• Calculated formula: C19 H56.97 N3 Si6 U
• Title of publication: Stable Uranium(VI) Methyl and Acetylide Complexes and the Elucidation of an Inverse Trans Influence Ligand Series
• Authors of publication: Andrew J. Lewis; Patrick J. Carroll; Eric J. Schelter
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 13185 - 13192
• a: 18.476 ± 0.004 Å
• b: 18.476 ± 0.004 Å
• c: 16.94 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5007.9 ± 1.9 ų
• Cell temperature: 143 ± 1 K
• Ambient diffraction temperature: 143 ± 1 K
• Number of distinct elements: 5
• Space group number: 161
• Hermann-Mauguin space group symbol: R 3 c :H
• Hall space group symbol: R 3 -2"c
• Residual factor for all reflections: 0.023
• Residual factor for significantly intense reflections: 0.021
• Weighted residual factors for significantly intense reflections: 0.0707
• Weighted residual factors for all reflections included in the refinement: 0.0868
• Goodness-of-fit parameter for all reflections included in the refinement: 1.386
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No