Information card for entry 4120790

Structure parameters

• Formula: C73.5 H55 B Cl3 Cu F24 P2 Sn2
• Calculated formula: C73.5 H55 B Cl3 Cu F24 P2 Sn2
• Title of publication: Activation of a σ-SnSn Bond at Copper, Followed by Double Addition to an Alkyne
• Authors of publication: Nicolas Lassauque; Pauline Gualco; Sonia Mallet-Ladeira; Karinne Miqueu; Abderrahmane Amgoune; Didier Bourissou
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 13827 - 13834
• a: 13.1739 ± 0.0009 Å
• b: 15.1534 ± 0.0011 Å
• c: 19.8524 ± 0.0013 Å
• α: 89.141 ± 0.003°
• β: 80.629 ± 0.003°
• γ: 88.954 ± 0.003°
• Cell volume: 3909.3 ± 0.5 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0518
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.0938
• Weighted residual factors for all reflections included in the refinement: 0.1042
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No