Information card for entry 4120791

Structure parameters

• Formula: C44 H48 Br Cu O P2 Sn2
• Calculated formula: C44 H48 Br Cu O P2 Sn2
• Title of publication: Activation of a σ-SnSn Bond at Copper, Followed by Double Addition to an Alkyne
• Authors of publication: Nicolas Lassauque; Pauline Gualco; Sonia Mallet-Ladeira; Karinne Miqueu; Abderrahmane Amgoune; Didier Bourissou
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 13827 - 13834
• a: 26.7541 ± 0.0015 Å
• b: 11.721 ± 0.0005 Å
• c: 27.3437 ± 0.0014 Å
• α: 90°
• β: 96.295 ± 0.002°
• γ: 90°
• Cell volume: 8522.9 ± 0.7 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0952
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.0686
• Weighted residual factors for all reflections included in the refinement: 0.0816
• Goodness-of-fit parameter for all reflections included in the refinement: 0.975
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No