Information card for entry 4120792

Structure parameters

• Formula: C78 H60 B Cl4 Cu F24 O2 P2 Sn2
• Calculated formula: C78 H60 B Cl4 Cu F24 O2 P2 Sn2
• Title of publication: Activation of a σ-SnSn Bond at Copper, Followed by Double Addition to an Alkyne
• Authors of publication: Nicolas Lassauque; Pauline Gualco; Sonia Mallet-Ladeira; Karinne Miqueu; Abderrahmane Amgoune; Didier Bourissou
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 13827 - 13834
• a: 20.154 ± 0.004 Å
• b: 13.161 ± 0.002 Å
• c: 31.163 ± 0.004 Å
• α: 90°
• β: 95.553 ± 0.005°
• γ: 90°
• Cell volume: 8227 ± 2 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0762
• Residual factor for significantly intense reflections: 0.0681
• Weighted residual factors for significantly intense reflections: 0.1546
• Weighted residual factors for all reflections included in the refinement: 0.1591
• Goodness-of-fit parameter for all reflections included in the refinement: 1.175
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No