Information card for entry 4121735

Structure parameters

• Formula: C51 H115 K O17 Si4 U
• Calculated formula: C51 H115 K O17 Si4 U
• Title of publication: Multimetallic Cooperativity in Uranium-Mediated CO2 Activation.
• Authors of publication: Cooper, Oliver; Camp, Clément; Pécaut, Jacques; Kefalidis, Christos E.; Maron, Laurent; Gambarelli, Serge; Mazzanti, Marinella
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 18
• Pages of publication: 6716 - 6723
• a: 13.5351 ± 0.0004 Å
• b: 13.6577 ± 0.0004 Å
• c: 23.083 ± 0.0007 Å
• α: 103.335 ± 0.002°
• β: 91.577 ± 0.002°
• γ: 118.941 ± 0.003°
• Cell volume: 3584.7 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0648
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.0749
• Weighted residual factors for all reflections included in the refinement: 0.0809
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No