Crystallography Open Database

Information card for entry 4121736

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Coordinates	4121736.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69.75 H142 K2 O25 Si4 U
Calculated formula	C69.75 H142 K2 O25 Si4 U
Title of publication	Multimetallic Cooperativity in Uranium-Mediated CO2 Activation.
Authors of publication	Cooper, Oliver; Camp, Clément; Pécaut, Jacques; Kefalidis, Christos E.; Maron, Laurent; Gambarelli, Serge; Mazzanti, Marinella
Journal of publication	Journal of the American Chemical Society
Year of publication	2014
Journal volume	136
Journal issue	18
Pages of publication	6716 - 6723
a	24.8819 ± 0.0009 Å
b	16.4764 ± 0.0005 Å
c	46.4053 ± 0.0012 Å
α	90°
β	92.983 ± 0.003°
γ	90°
Cell volume	18998.7 ± 1 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1468
Residual factor for significantly intense reflections	0.0983
Weighted residual factors for significantly intense reflections	0.1447
Weighted residual factors for all reflections included in the refinement	0.1608
Goodness-of-fit parameter for all reflections included in the refinement	1.323
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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