Information card for entry 4122050

Structure parameters

• Formula: C102 H158 K2 N4 O4 Si4
• Calculated formula: C102 H158 K2 N4 O4 Si4
• Title of publication: One-electron-mediated rearrangements of 2,3-disiladicarbene.
• Authors of publication: Mondal, Kartik Chandra; Samuel, Prinson P.; Roesky, Herbert W.; Aysin, Rinat R.; Leites, Larissa A.; Neudeck, Sven; Lübben, Jens; Dittrich, Birger; Holzmann, Nicole; Hermann, Markus; Frenking, Gernot
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 25
• Pages of publication: 8919 - 8922
• a: 12.0658 ± 0.0006 Å
• b: 23.2378 ± 0.0012 Å
• c: 17.4312 ± 0.0009 Å
• α: 90°
• β: 97.8342 ± 0.0013°
• γ: 90°
• Cell volume: 4841.8 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.056
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for significantly intense reflections: 0.1276
• Weighted residual factors for all reflections included in the refinement: 0.1364
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No