Information card for entry 4122051

Structure parameters

• Formula: C46 H70 N2 Si2
• Calculated formula: C46 H70 N2 Si2
• Title of publication: One-electron-mediated rearrangements of 2,3-disiladicarbene.
• Authors of publication: Mondal, Kartik Chandra; Samuel, Prinson P.; Roesky, Herbert W.; Aysin, Rinat R.; Leites, Larissa A.; Neudeck, Sven; Lübben, Jens; Dittrich, Birger; Holzmann, Nicole; Hermann, Markus; Frenking, Gernot
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 25
• Pages of publication: 8919 - 8922
• a: 12.79 ± 0.02 Å
• b: 13.783 ± 0.009 Å
• c: 14.433 ± 0.019 Å
• α: 66.35 ± 0.06°
• β: 79.58 ± 0.1°
• γ: 67.48 ± 0.07°
• Cell volume: 2152 ± 5 ų
• Cell temperature: 23 ± 2 K
• Ambient diffraction temperature: 23 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1285
• Residual factor for significantly intense reflections: 0.0641
• Weighted residual factors for significantly intense reflections: 0.1418
• Weighted residual factors for all reflections included in the refinement: 0.1721
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.4769 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No