Crystallography Open Database

Information card for entry 4122691

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Coordinates	4122691.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H50 N6 Si2
Calculated formula	C32 H50 N6 Si2
Title of publication	An Amplified Ylidic "Half-Parent" Iminosilane LSi═NH.
Authors of publication	Hansen, Kerstin; Szilvási, Tibor; Blom, Burgert; Driess, Matthias
Journal of publication	Journal of the American Chemical Society
Year of publication	2014
Journal volume	136
Journal issue	40
Pages of publication	14207
a	9.0265 ± 0.0002 Å
b	19.804 ± 0.0004 Å
c	10.3399 ± 0.0003 Å
α	90°
β	114.806 ± 0.003°
γ	90°
Cell volume	1677.83 ± 0.08 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	4
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0759
Residual factor for significantly intense reflections	0.0722
Weighted residual factors for significantly intense reflections	0.1848
Weighted residual factors for all reflections included in the refinement	0.1878
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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