Information card for entry 4124459

Structure parameters

• Formula: C76 H75 B F24 Ge N2 O3 Si W
• Calculated formula: C76 H75 B F24 Ge N2 O3 Si W
• Title of publication: Insertion of a Cationic Metallogermylene into E-H Bonds (E = H, B, Si).
• Authors of publication: Inomata, Koya; Watanabe, Takahito; Miyazaki, Yoshikazu; Tobita, Hiromi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Journal volume: 137
• Journal issue: 37
• Pages of publication: 11935 - 11937
• a: 16.2451 ± 0.0005 Å
• b: 22.0047 ± 0.0009 Å
• c: 25.4722 ± 0.001 Å
• α: 64.8116 ± 0.001°
• β: 77.7275 ± 0.0007°
• γ: 76.6013 ± 0.0007°
• Cell volume: 7948 ± 0.5 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1049
• Residual factor for significantly intense reflections: 0.0732
• Weighted residual factors for significantly intense reflections: 0.1629
• Weighted residual factors for all reflections included in the refinement: 0.1798
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No