Information card for entry 4128137

Structure parameters

• Formula: C16 H32 K O P Si2
• Calculated formula: C16 H32 K O P Si2
• Title of publication: Direct Functionalization of White Phosphorus to Cyclotetraphosphanes: Selective Formation of Four P-C Bonds.
• Authors of publication: Du, Shanshan; Yang, Jimin; Hu, Jingyuan; Chai, Zhengqi; Luo, Gen; Luo, Yi; Zhang, Wen-Xiong; Xi, Zhenfeng
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 17
• Pages of publication: 6843 - 6847
• a: 15.9907 ± 0.0014 Å
• b: 12.3762 ± 0.0011 Å
• c: 10.9542 ± 0.0009 Å
• α: 90°
• β: 95.493 ± 0.007°
• γ: 90°
• Cell volume: 2157.9 ± 0.3 ų
• Cell temperature: 179.9 ± 0.4 K
• Ambient diffraction temperature: 179.9 ± 0.4 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0996
• Residual factor for significantly intense reflections: 0.0655
• Weighted residual factors for significantly intense reflections: 0.1299
• Weighted residual factors for all reflections included in the refinement: 0.1429
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No