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Information card for entry 4128137
Preview
Coordinates | 4128137.cif |
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Original paper (by DOI) | HTML |
Formula | C16 H32 K O P Si2 |
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Calculated formula | C16 H32 K O P Si2 |
Title of publication | Direct Functionalization of White Phosphorus to Cyclotetraphosphanes: Selective Formation of Four P-C Bonds. |
Authors of publication | Du, Shanshan; Yang, Jimin; Hu, Jingyuan; Chai, Zhengqi; Luo, Gen; Luo, Yi; Zhang, Wen-Xiong; Xi, Zhenfeng |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2019 |
Journal volume | 141 |
Journal issue | 17 |
Pages of publication | 6843 - 6847 |
a | 15.9907 ± 0.0014 Å |
b | 12.3762 ± 0.0011 Å |
c | 10.9542 ± 0.0009 Å |
α | 90° |
β | 95.493 ± 0.007° |
γ | 90° |
Cell volume | 2157.9 ± 0.3 Å3 |
Cell temperature | 179.9 ± 0.4 K |
Ambient diffraction temperature | 179.9 ± 0.4 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0996 |
Residual factor for significantly intense reflections | 0.0655 |
Weighted residual factors for significantly intense reflections | 0.1299 |
Weighted residual factors for all reflections included in the refinement | 0.1429 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4128137.html
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Users of the data should acknowledge the original authors of the
structural data.