Information card for entry 4129818

Structure parameters

• Common name: KH-1484
• Chemical name: toste130
• Formula: C30 H26 Cl O3 P
• Calculated formula: C30 H26 Cl O3 P
• Title of publication: Phosphonium Formation by Facile Carbon-Phosphorus Reductive Elimination from Gold(III).
• Authors of publication: Kawai, Hiroyuki; Wolf, William J.; DiPasquale, Antonio G.; Winston, Matthew S.; Toste, F. Dean
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 2
• Pages of publication: 587 - 593
• a: 8.6367 ± 0.0006 Å
• b: 11.9128 ± 0.0008 Å
• c: 12.4392 ± 0.0008 Å
• α: 103.096 ± 0.001°
• β: 91.766 ± 0.002°
• γ: 103.918 ± 0.001°
• Cell volume: 1205.01 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0791
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections included in the refinement: 0.0984
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No