Information card for entry 4130892

Structure parameters

• Formula: C83 H117 Ge N2 Si2
• Calculated formula: C83 H117 Ge N2 Si2
• Title of publication: Regiodiscriminating Reactivity of Isolable NHC-Coordinated Disilenyl Germylene and Its Cyclic Isomer.
• Authors of publication: Nieder, David; Huch, Volker; Yildiz, Cem B.; Scheschkewitz, David
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 42
• Pages of publication: 13996 - 14005
• a: 15.9617 ± 0.0017 Å
• b: 16.6009 ± 0.0018 Å
• c: 17.9948 ± 0.0019 Å
• α: 114.148 ± 0.005°
• β: 112.883 ± 0.005°
• γ: 96.575 ± 0.005°
• Cell volume: 3790.4 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0672
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.1414
• Weighted residual factors for all reflections included in the refinement: 0.1525
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No