Crystallography Open Database

Information card for entry 4130893

Preview

Coordinates	4130893.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C77 H108 Ge N2 Si2
Calculated formula	C77 H108 Ge N2 Si2
Title of publication	Regiodiscriminating Reactivity of Isolable NHC-Coordinated Disilenyl Germylene and Its Cyclic Isomer.
Authors of publication	Nieder, David; Huch, Volker; Yildiz, Cem B.; Scheschkewitz, David
Journal of publication	Journal of the American Chemical Society
Year of publication	2016
Journal volume	138
Journal issue	42
Pages of publication	13996 - 14005
a	11.4319 ± 0.0005 Å
b	14.6466 ± 0.0005 Å
c	21.5014 ± 0.0009 Å
α	100.512 ± 0.001°
β	92.045 ± 0.001°
γ	95.265 ± 0.001°
Cell volume	3519.7 ± 0.2 Å³
Cell temperature	163 ± 2 K
Ambient diffraction temperature	163 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0533
Residual factor for significantly intense reflections	0.0385
Weighted residual factors for significantly intense reflections	0.0941
Weighted residual factors for all reflections included in the refinement	0.1015
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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