Information card for entry 4130894

Structure parameters

• Formula: C76.25 H115 Ge N2 Si2
• Calculated formula: C76.25 H112 Ge N2 Si2
• Title of publication: Regiodiscriminating Reactivity of Isolable NHC-Coordinated Disilenyl Germylene and Its Cyclic Isomer.
• Authors of publication: Nieder, David; Huch, Volker; Yildiz, Cem B.; Scheschkewitz, David
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 42
• Pages of publication: 13996 - 14005
• a: 12.6352 ± 0.0003 Å
• b: 23.8472 ± 0.0006 Å
• c: 25.5287 ± 0.0007 Å
• α: 90°
• β: 101.535 ± 0.001°
• γ: 90°
• Cell volume: 7536.8 ± 0.3 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0789
• Residual factor for significantly intense reflections: 0.0571
• Weighted residual factors for significantly intense reflections: 0.1648
• Weighted residual factors for all reflections included in the refinement: 0.1777
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No