Information card for entry 4133284

Structure parameters

• Formula: C49 H55 B Ge K O7 P
• Calculated formula: C49 H55 B Ge K O7 P
• Title of publication: P, P-Dimethylformylphosphine: The Phosphorus Analogue of N, N-Dimethylformamide.
• Authors of publication: Szkop, Kevin M.; Jupp, Andrew R.; Stephan, Douglas W.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 40
• Pages of publication: 12751 - 12755
• a: 25.154 ± 0.002 Å
• b: 11.917 ± 0.0009 Å
• c: 15.3471 ± 0.0011 Å
• α: 90°
• β: 98.553 ± 0.007°
• γ: 90°
• Cell volume: 4549.3 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1347
• Residual factor for significantly intense reflections: 0.0767
• Weighted residual factors for significantly intense reflections: 0.1954
• Weighted residual factors for all reflections included in the refinement: 0.2087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No