Crystallography Open Database

Information card for entry 4133285

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Coordinates	4133285.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C13 H20.67 Cl2 O P Ru
Calculated formula	C13 H20.6667 Cl2 O P Ru
Title of publication	P, P-Dimethylformylphosphine: The Phosphorus Analogue of N, N-Dimethylformamide.
Authors of publication	Szkop, Kevin M.; Jupp, Andrew R.; Stephan, Douglas W.
Journal of publication	Journal of the American Chemical Society
Year of publication	2018
Journal volume	140
Journal issue	40
Pages of publication	12751 - 12755
a	6.4177 ± 0.0003 Å
b	28.9354 ± 0.0015 Å
c	25.7657 ± 0.0014 Å
α	90°
β	92.35 ± 0.002°
γ	90°
Cell volume	4780.6 ± 0.4 Å³
Cell temperature	423 ± 2 K
Ambient diffraction temperature	423 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0428
Residual factor for significantly intense reflections	0.0375
Weighted residual factors for significantly intense reflections	0.0778
Weighted residual factors for all reflections included in the refinement	0.0796
Goodness-of-fit parameter for all reflections included in the refinement	1.172
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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