Information card for entry 4133625

Structure parameters

• Formula: C51 H68 N4 O4 Si2
• Calculated formula: C51 H68 N4 O4 Si2
• Title of publication: Silicon-Mediated Selective Homo- and Heterocoupling of Carbon Monoxide.
• Authors of publication: Wang, Yuwen; Kostenko, Arseni; Hadlington, Terrance J.; Luecke, Marcel-Philip; Yao, Shenglai; Driess, Matthias
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 1
• Pages of publication: 626 - 634
• a: 15.6523 ± 0.0002 Å
• b: 17.3543 ± 0.0003 Å
• c: 18.3413 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4982.13 ± 0.12 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0606
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.1167
• Weighted residual factors for all reflections included in the refinement: 0.1277
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No