Information card for entry 4134378

Structure parameters

• Formula: C168 H198 Cl4 Ge4 N16 O
• Calculated formula: C168 H198 Cl4 Ge4 N16 O
• Title of publication: Ge(0) Compound Stabilized by a Diimino-Carbene Ligand: Synthesis and Ambiphilic Reactivity.
• Authors of publication: Nguyen, Minh Tho; Gusev, Dmitry; Dmitrienko, Anton; Gabidullin, Bulat M.; Spasyuk, Denis; Pilkington, Melanie; Nikonov, Georgii I.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• Journal volume: 142
• Journal issue: 12
• Pages of publication: 5852 - 5861
• a: 8.8382 ± 0.0007 Å
• b: 15.3641 ± 0.0016 Å
• c: 28.9948 ± 0.0019 Å
• α: 92.772 ± 0.006°
• β: 97.63 ± 0.003°
• γ: 96.14 ± 0.004°
• Cell volume: 3872.2 ± 0.6 ų
• Cell temperature: 152 ± 2 K
• Ambient diffraction temperature: 152.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1007
• Residual factor for significantly intense reflections: 0.0838
• Weighted residual factors for significantly intense reflections: 0.197
• Weighted residual factors for all reflections included in the refinement: 0.2073
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No