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Information card for entry 4135061
Preview
Coordinates | 4135061.cif |
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Original paper (by DOI) | HTML |
Formula | C29 H25 Ge N O2 |
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Calculated formula | C29 H25 Ge N O2 |
Title of publication | Ligand-Controlled Regiodivergent Palladium-Catalyzed Hydrogermylation of Ynamides. |
Authors of publication | Debrauwer, Vincent; Turlik, Aneta; Rummler, Lénaic; Prescimone, Alessandro; Blanchard, Nicolas; Houk, K. N.; Bizet, Vincent |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2020 |
Journal volume | 142 |
Journal issue | 25 |
Pages of publication | 11153 - 11164 |
a | 10.3008 ± 0.0008 Å |
b | 10.3151 ± 0.0009 Å |
c | 13.5595 ± 0.0014 Å |
α | 94.497 ± 0.008° |
β | 103.341 ± 0.007° |
γ | 119.914 ± 0.006° |
Cell volume | 1182.7 ± 0.2 Å3 |
Cell temperature | 123 K |
Ambient diffraction temperature | 123 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0511 |
Residual factor for significantly intense reflections | 0.0461 |
Weighted residual factors for all reflections | 0.064 |
Weighted residual factors for significantly intense reflections | 0.0569 |
Weighted residual factors for all reflections included in the refinement | 0.0583 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.0623 |
Diffraction radiation wavelength | 1.34143 Å |
Diffraction radiation type | GaKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4135061.html
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