Information card for entry 4135062

Structure parameters

• Formula: C30 H27 Ge N O3
• Calculated formula: C30 H27 Ge N O3
• Title of publication: Ligand-Controlled Regiodivergent Palladium-Catalyzed Hydrogermylation of Ynamides.
• Authors of publication: Debrauwer, Vincent; Turlik, Aneta; Rummler, Lénaic; Prescimone, Alessandro; Blanchard, Nicolas; Houk, K. N.; Bizet, Vincent
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• Journal volume: 142
• Journal issue: 25
• Pages of publication: 11153 - 11164
• a: 20.0288 ± 0.0008 Å
• b: 14.5601 ± 0.0007 Å
• c: 18.7951 ± 0.0008 Å
• α: 90°
• β: 115.273 ± 0.002°
• γ: 90°
• Cell volume: 4956.4 ± 0.4 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for significantly intense reflections: 0.0994
• Weighted residual factors for all reflections included in the refinement: 0.1034
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No